Recovery of phenolic compounds from grape seeds: effect of extraction time and solid-liquid ratio.
Identifieur interne : 000A67 ( Main/Exploration ); précédent : 000A66; suivant : 000A68Recovery of phenolic compounds from grape seeds: effect of extraction time and solid-liquid ratio.
Auteurs : Alessandro A. Casazza [Italie] ; Bahar Aliakbarian ; Patrizia PeregoSource :
- Natural product research ; 2011.
English descriptors
- KwdEn :
- Biphenyl Compounds (metabolism), Chromatography, High Pressure Liquid, Ethanol, Flavonoids (analysis), Flavonoids (isolation & purification), Grape Seed Extract (analysis), Grape Seed Extract (isolation & purification), Grape Seed Extract (pharmacology), Picrates (metabolism), Polyphenols (analysis), Polyphenols (isolation & purification), Polyphenols (pharmacology), Seeds (chemistry), Time Factors, Vitis (chemistry).
- MESH :
- chemical , analysis : Flavonoids, Grape Seed Extract, Polyphenols.
- chemical , isolation & purification : Flavonoids, Grape Seed Extract, Polyphenols.
- chemical , metabolism : Biphenyl Compounds, Picrates.
- chemical , pharmacology : Grape Seed Extract, Polyphenols.
- chemistry : Seeds, Vitis.
- Chromatography, High Pressure Liquid, Ethanol, Time Factors.
Abstract
The aim of this research was to study the recovery of phenolic compounds from grape seeds, by-products from winemaking industries, using ethanolic solid-liquid extraction. For such a purpose, the combined effects of the extraction time (9, 19 and 29 h) and the solid-liquid ratio (0.10, 0.20 and 0.30 gdw mL(-1)), were investigated (where dw = dry waste). Results demonstrated that Pinot Noir seeds had high levels of both total polyphenols (73.66 mg(Gallic Acid Equivalent) gdw(-1)) and flavonoids (30.90 mg(Catechin Equivalent) gdw(-1)), being the optimum extraction time 19 h approximately. The main phenolic compounds analysed with high performance liquid chromatography were catechin and quercetin with a maximum extraction yield obtained at 29 h (362.23 and 339.35 mg/100 gdw, respectively). Concentration of the polyphenols and their antiradical powers are demonstrated to have a significant linear correlation.
DOI: 10.1080/14786419.2010.524889
PubMed: 21707256
Affiliations:
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Le document en format XML
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<author><name sortKey="Casazza, Alessandro A" sort="Casazza, Alessandro A" uniqKey="Casazza A" first="Alessandro A" last="Casazza">Alessandro A. Casazza</name>
<affiliation wicri:level="1"><nlm:affiliation>Department of Chemical and Process Engineering G.B. Bonino, University of Genoa, Via Opera Pia 15, 16145 Genoa, Italy. alessandro.casazza@unige.it</nlm:affiliation>
<country xml:lang="fr">Italie</country>
<wicri:regionArea>Department of Chemical and Process Engineering G.B. Bonino, University of Genoa, Via Opera Pia 15, 16145 Genoa</wicri:regionArea>
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<author><name sortKey="Aliakbarian, Bahar" sort="Aliakbarian, Bahar" uniqKey="Aliakbarian B" first="Bahar" last="Aliakbarian">Bahar Aliakbarian</name>
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<sourceDesc><biblStruct><analytic><title xml:lang="en">Recovery of phenolic compounds from grape seeds: effect of extraction time and solid-liquid ratio.</title>
<author><name sortKey="Casazza, Alessandro A" sort="Casazza, Alessandro A" uniqKey="Casazza A" first="Alessandro A" last="Casazza">Alessandro A. Casazza</name>
<affiliation wicri:level="1"><nlm:affiliation>Department of Chemical and Process Engineering G.B. Bonino, University of Genoa, Via Opera Pia 15, 16145 Genoa, Italy. alessandro.casazza@unige.it</nlm:affiliation>
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<author><name sortKey="Aliakbarian, Bahar" sort="Aliakbarian, Bahar" uniqKey="Aliakbarian B" first="Bahar" last="Aliakbarian">Bahar Aliakbarian</name>
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<series><title level="j">Natural product research</title>
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<term>Ethanol</term>
<term>Flavonoids (analysis)</term>
<term>Flavonoids (isolation & purification)</term>
<term>Grape Seed Extract (analysis)</term>
<term>Grape Seed Extract (isolation & purification)</term>
<term>Grape Seed Extract (pharmacology)</term>
<term>Picrates (metabolism)</term>
<term>Polyphenols (analysis)</term>
<term>Polyphenols (isolation & purification)</term>
<term>Polyphenols (pharmacology)</term>
<term>Seeds (chemistry)</term>
<term>Time Factors</term>
<term>Vitis (chemistry)</term>
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<keywords scheme="MESH" type="chemical" qualifier="analysis" xml:lang="en"><term>Flavonoids</term>
<term>Grape Seed Extract</term>
<term>Polyphenols</term>
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<keywords scheme="MESH" type="chemical" qualifier="isolation & purification" xml:lang="en"><term>Flavonoids</term>
<term>Grape Seed Extract</term>
<term>Polyphenols</term>
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<term>Picrates</term>
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<term>Vitis</term>
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<term>Ethanol</term>
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<front><div type="abstract" xml:lang="en">The aim of this research was to study the recovery of phenolic compounds from grape seeds, by-products from winemaking industries, using ethanolic solid-liquid extraction. For such a purpose, the combined effects of the extraction time (9, 19 and 29 h) and the solid-liquid ratio (0.10, 0.20 and 0.30 gdw mL(-1)), were investigated (where dw = dry waste). Results demonstrated that Pinot Noir seeds had high levels of both total polyphenols (73.66 mg(Gallic Acid Equivalent) gdw(-1)) and flavonoids (30.90 mg(Catechin Equivalent) gdw(-1)), being the optimum extraction time 19 h approximately. The main phenolic compounds analysed with high performance liquid chromatography were catechin and quercetin with a maximum extraction yield obtained at 29 h (362.23 and 339.35 mg/100 gdw, respectively). Concentration of the polyphenols and their antiradical powers are demonstrated to have a significant linear correlation.</div>
</front>
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<name sortKey="Perego, Patrizia" sort="Perego, Patrizia" uniqKey="Perego P" first="Patrizia" last="Perego">Patrizia Perego</name>
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<country name="Italie"><noRegion><name sortKey="Casazza, Alessandro A" sort="Casazza, Alessandro A" uniqKey="Casazza A" first="Alessandro A" last="Casazza">Alessandro A. Casazza</name>
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